Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones

GÜP, Ramazan; KOÇ, ZIYA ERDEM

Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones

Ramazan GÜP, (Muğla Üniversitesi, Fen Edebiyat Fakültesi, Kimya Bölümü, Muğla, Türkiye)

Ziya Erdem KOÇ (Girilmedi)

Selçuk Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi

1 0

Yıl: 2004 Cilt: 0 Sayı: 23 Sayfa Aralığı: 15 - 19 Metin Dili: Türkçe İndeks Tarihi: 29-07-2022

Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones

Öz:

Bu çalışmada, 4-aminobenzoik asit hidrazinin 4-metilasetofenon, 4-kloroasetofenon ve isonitrosoasetofenon ile reaksiyonundan sırasıyla 4-metilasetofenon 4-aminobenzoil hidrazon $(L_1)$, 4-kloroasetofenon 4-aminobenzoil hidrazon $(L_2)$ ve isonitrosoasetofenon 4-aminobenzoil hidrazon $(L_3)$ bileşikleri sentezlenmiştir. Bu yeni bileşiklerin yapıları $^{1}H-NMR$, IR ve elementel analiz teknikleri kullanılarak aydınlatılmıştır. Ayrıca bu bileşiklerin Ni(ll), Cu(ll), Co(ll), Zn(ll), Mn(ll) ve Cd(ll) iyonları ile katı-sıvı ekstraksiyon özellikleri incelenmiştir.

Anahtar Kelime:

4-metilasetofenon 4-aminobenzoil hidrazon, 4-kloroasetofenon 4-aminobenzoil hidrazon ve isonitrosoasetofenon 4-aminobenzoil hidrazon'un sentezi ve ekstraksiyon özelliklerinin incelenmesi

Öz:

4-Methylacetophenone p-aminobenzoylhydrazone $(L_1)$,4-chloroacetophenone p-aminobenzoylhydrazone $(L_2)$ and isonitrosoacetophenone p-aminobenzoylhydrazone $(L_3)$ were prepared by reaction of 4-aminobenzoic acid hyrazide with p-methylacetophenone, p-chloroacetophenone and isonitrosoacetophenone, respectively. The structures of these new compounds were proposed on the basis of elemental analysis, $^{1}H-NMR$ and IR data. The extraction abilities of these new compounds were also examined by the solid-liquid extraction of selected transition metal [ Ni(ll), Cu(ll), Co(ll), Zn(ll), Mn(ll) and Cd(ll)] ions.

Anahtar Kelime:

Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık

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APA	GÜP R, KOÇ Z (2004). Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones. , 15 - 19.
Chicago	GÜP Ramazan,KOÇ ZIYA ERDEM Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones. (2004): 15 - 19.
MLA	GÜP Ramazan,KOÇ ZIYA ERDEM Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones. , 2004, ss.15 - 19.
AMA	GÜP R,KOÇ Z Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones. . 2004; 15 - 19.
Vancouver	GÜP R,KOÇ Z Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones. . 2004; 15 - 19.
IEEE	GÜP R,KOÇ Z "Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones." , ss.15 - 19, 2004.
ISNAD	GÜP, Ramazan - KOÇ, ZIYA ERDEM. "Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones". (2004), 15-19.

APA	GÜP R, KOÇ Z (2004). Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones. Selçuk Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi, 0(23), 15 - 19.
Chicago	GÜP Ramazan,KOÇ ZIYA ERDEM Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones. Selçuk Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi 0, no.23 (2004): 15 - 19.
MLA	GÜP Ramazan,KOÇ ZIYA ERDEM Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones. Selçuk Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi, vol.0, no.23, 2004, ss.15 - 19.
AMA	GÜP R,KOÇ Z Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones. Selçuk Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi. 2004; 0(23): 15 - 19.
Vancouver	GÜP R,KOÇ Z Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones. Selçuk Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi. 2004; 0(23): 15 - 19.
IEEE	GÜP R,KOÇ Z "Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones." Selçuk Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi, 0, ss.15 - 19, 2004.
ISNAD	GÜP, Ramazan - KOÇ, ZIYA ERDEM. "Synthesis and investigation extraction properties of 4- methylacetophenone, 4-chloroacetophenone and isonitrosoacetephenone 4-aminobenzoylhydrazones". Selçuk Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi 23 (2004), 15-19.