Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez

AKŞİT, ZEYNEP; Baltaci, Cemalettin

Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez

Cemalettin BALTACI, (Gümüşhane Üniversitesi, Gıda Mühendisliği Bölümü, Gümüşhane, Türkiye)

Zeynep AKŞİT (Gümüşhane Üniversitesi, Gıda Mühendisliği Bölümü, Gümüşhane, Türkiye)

Hittite Journal of Science and Engineering

7 1

Yıl: 2016 Cilt: 3 Sayı: 2 Sayfa Aralığı: 91 - 97 Metin Dili: İngilizce İndeks Tarihi: 29-07-2022

Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez

Öz:

T his study represents a high performance liquid chromatography (HPLC) method for the detection of 5-hydroxymethylfurfural in pestil, köme, jam and pekmez samples. The linearity, selectivity, decision limit, detection capability, detection limit, quantification limit, precision, recovery, ruggedness and measurement uncertainty of the method were determined. The developed method, simple and accurate, showed good recovery values (97-108%). The accuracy of the method expressed with the relative standard deviation was below 6%. The detection limit and quantification limit were 0.03 mg/kg and 0.10 mg/kg, respectively. HMF levels in pestil, köme, jam, marmalade and pekmez samples were determined using the validated method

Anahtar Kelime:

Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık

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APA	Baltaci C, AKŞİT Z (2016). Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez. , 91 - 97.
Chicago	Baltaci Cemalettin,AKŞİT ZEYNEP Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez. (2016): 91 - 97.
MLA	Baltaci Cemalettin,AKŞİT ZEYNEP Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez. , 2016, ss.91 - 97.
AMA	Baltaci C,AKŞİT Z Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez. . 2016; 91 - 97.
Vancouver	Baltaci C,AKŞİT Z Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez. . 2016; 91 - 97.
IEEE	Baltaci C,AKŞİT Z "Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez." , ss.91 - 97, 2016.
ISNAD	Baltaci, Cemalettin - AKŞİT, ZEYNEP. "Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez". (2016), 91-97.

APA	Baltaci C, AKŞİT Z (2016). Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez. Hittite Journal of Science and Engineering, 3(2), 91 - 97.
Chicago	Baltaci Cemalettin,AKŞİT ZEYNEP Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez. Hittite Journal of Science and Engineering 3, no.2 (2016): 91 - 97.
MLA	Baltaci Cemalettin,AKŞİT ZEYNEP Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez. Hittite Journal of Science and Engineering, vol.3, no.2, 2016, ss.91 - 97.
AMA	Baltaci C,AKŞİT Z Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez. Hittite Journal of Science and Engineering. 2016; 3(2): 91 - 97.
Vancouver	Baltaci C,AKŞİT Z Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez. Hittite Journal of Science and Engineering. 2016; 3(2): 91 - 97.
IEEE	Baltaci C,AKŞİT Z "Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez." Hittite Journal of Science and Engineering, 3, ss.91 - 97, 2016.
ISNAD	Baltaci, Cemalettin - AKŞİT, ZEYNEP. "Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade And Pekmez". Hittite Journal of Science and Engineering 3/2 (2016), 91-97.