Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor

AL, Selgin

Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor

Selgin AL (Ahi Evran Üniversitesi, Fen Edebiyat Fakültesi, Fizik Bölümü, Kırşehir)

Balıkesir Üniversitesi Fen Bilimleri Enstitüsü Dergisi

3 2

Yıl: 2017 Cilt: 19 Sayı: 3 Sayfa Aralığı: 58 - 63 Metin Dili: Türkçe İndeks Tarihi: 29-07-2022

Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor

Öz:

ABO3 perovskite ailesinden olan seramik esaslı malzemeler, gaz ortamına bağlı olarak orta sıcaklıklarda (500-800°C) hem proton hem de oksijen iyonu iletkenlita şıma özelliklerinden ve bunların orta sıcaklık katı oksit yakıt pillerinde elektrolit olarak kullanılma potansiyellerinden dolayı ilgi çekmitip proton iletken malzeme sentezlenmiştir. X-ışını difraksiyonu (XRD) ve X-ışını enerji dağılımı spektrometresi (EDXS) karakterizasyon teknikleri kullanılarak toz formundaki malzemenin kristalografik yapısı, faz saflıveri tabanı ile karşılaştırılmış olup, standart perovskite yapısı ile mükemmel uyum göstermiştir. Yüzey alanı ölçümü Brunauer-Emmett-Teller (BET) yöntemi kullanılarak gerçekleştirildi. İletkenlik ölçümü, farklı gaz ortamlarında AC empedansı kullanılarak orta sıcaklık aralığında gerçekleştirildi

Anahtar Kelime:

Perovskit tipi proton ileten bir malzemenin sentezi, karakterizasyonu ve iletkenlik ölçümü

Öz:

Ceramic based materials from the ABO3 perovskite family, show both proton and oxide ion conductivity at intermediate temperatures depending on the gaseous environment. Due to these multi-species transport features of them and their potential to be utilised as an electrolyte in solid oxide fuel cells operating at intermediate temperature, there has been lot of research focused on them and their properties. In this study, a perovskite type proton conductor was synthesised by using solid state reaction method. X-ray diffraction (XRD) and Energy dispersive X-ray spectroscopy (EDXS) characterisation techniques were utilised to determine crystal structure, phase purity and the elemental materials composition in powder form. The results were compared with International Centre for Diffraction Data (ICDD) database and displayed excellent match with standard perovskite structure. Also, the surface area measurement was performed via utilising the Brunauer-Emmett-Teller (BET) method. The conductivity measurement was carried out at the intermediate temperature (500-800°C) using AC impedance at different atmospheres

Anahtar Kelime:

Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık

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APA	AL S (2017). Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor. , 58 - 63.
Chicago	AL Selgin Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor. (2017): 58 - 63.
MLA	AL Selgin Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor. , 2017, ss.58 - 63.
AMA	AL S Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor. . 2017; 58 - 63.
Vancouver	AL S Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor. . 2017; 58 - 63.
IEEE	AL S "Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor." , ss.58 - 63, 2017.
ISNAD	AL, Selgin. "Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor". (2017), 58-63.

APA	AL S (2017). Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor. Balıkesir Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 19(3), 58 - 63.
Chicago	AL Selgin Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor. Balıkesir Üniversitesi Fen Bilimleri Enstitüsü Dergisi 19, no.3 (2017): 58 - 63.
MLA	AL Selgin Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor. Balıkesir Üniversitesi Fen Bilimleri Enstitüsü Dergisi, vol.19, no.3, 2017, ss.58 - 63.
AMA	AL S Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor. Balıkesir Üniversitesi Fen Bilimleri Enstitüsü Dergisi. 2017; 19(3): 58 - 63.
Vancouver	AL S Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor. Balıkesir Üniversitesi Fen Bilimleri Enstitüsü Dergisi. 2017; 19(3): 58 - 63.
IEEE	AL S "Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor." Balıkesir Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 19, ss.58 - 63, 2017.
ISNAD	AL, Selgin. "Fabrication, characterisation and conductivity measurement of a perovskite-type proton conductor". Balıkesir Üniversitesi Fen Bilimleri Enstitüsü Dergisi 19/3 (2017), 58-63.