Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry

TİTRETİR DURAN, Serap

Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry

Serap TİTRETİR DURAN (İnönü Üniversitesi)

Gazi University Journal of Science

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Yıl: 2019 Cilt: 32 Sayı: 2 Sayfa Aralığı: 426 - 438 Metin Dili: İngilizce İndeks Tarihi: 20-02-2020

Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry

Öz:

Bisphenol A (BPA) is important matter in chemical industry used in the produce of some foodcontact materials such as plastics, adhesives and coatings. But BPA has also some toxic effectsfor human endocrine system and environment. Therefore, novel sensitive and selective methodsfor determination the level of BPA in environmental, medical samples and foods newmeasurement methods need to be developed. A novel, sensitive, simple and cheapelectrochemical sensor based on poly (p-aminobenzoic acid) p(p-ABA) modified gold electrode(AuE) was developed for the measurement of BPA in water samples. Firstly, AuEs were modifiedwith polymerization of the p-amino benzoic acid as a monomer by using bulk electrolysis in 0.01M HCl at -250 mV. Then the electrochemical oxidation of BPA carried out in 0.1 M phosphatebuffer solution (PBS) pH=6 on p(p-ABA) modified AuE. The effects of various electrochemicalparameters, such as scan rate, electroyte type and electrolyte pH were examined. Differentialpulse voltammetry (DPV) was used as an ideal analytical method for the qualitative andquantitative detect of BPA in water samples. The developed electrochemical sensor has linearsignal to BPA in the range of 2–100 μM. Prepared electrode was showed the limit of detection(LOD) of 0.26 µM and R2 of 0.999. Additionally, the developed sensor s used to determinationthe BPA in bottled drinking water sold in Turkish markets by using DPV, and obtains satisfactoryresults. The recovery values of the bottle water samples in the freezer, at room temperature andin the car were calculated as 102.22%, 104.68% and 106.06% respectively.

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APA	TİTRETİR DURAN S (2019). Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry. , 426 - 438.
Chicago	TİTRETİR DURAN Serap Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry. (2019): 426 - 438.
MLA	TİTRETİR DURAN Serap Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry. , 2019, ss.426 - 438.
AMA	TİTRETİR DURAN S Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry. . 2019; 426 - 438.
Vancouver	TİTRETİR DURAN S Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry. . 2019; 426 - 438.
IEEE	TİTRETİR DURAN S "Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry." , ss.426 - 438, 2019.
ISNAD	TİTRETİR DURAN, Serap. "Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry". (2019), 426-438.

APA	TİTRETİR DURAN S (2019). Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry. Gazi University Journal of Science, 32(2), 426 - 438.
Chicago	TİTRETİR DURAN Serap Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry. Gazi University Journal of Science 32, no.2 (2019): 426 - 438.
MLA	TİTRETİR DURAN Serap Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry. Gazi University Journal of Science, vol.32, no.2, 2019, ss.426 - 438.
AMA	TİTRETİR DURAN S Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry. Gazi University Journal of Science. 2019; 32(2): 426 - 438.
Vancouver	TİTRETİR DURAN S Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry. Gazi University Journal of Science. 2019; 32(2): 426 - 438.
IEEE	TİTRETİR DURAN S "Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry." Gazi University Journal of Science, 32, ss.426 - 438, 2019.
ISNAD	TİTRETİR DURAN, Serap. "Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry". Gazi University Journal of Science 32/2 (2019), 426-438.