Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass
Yıl: 2020 Cilt: 7 Sayı: 2 Sayfa Aralığı: 127 - 131 Metin Dili: İngilizce DOI: 10.30897/ijegeo.700599 İndeks Tarihi: 21-10-2020
Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass
Öz: Synthesize of low price stationary phases with permanent groups for reversed-phase liquid chromatography (RP-HPLC) has gained great importance in the past several years. In chromatographic analyses, silica gels are commonly used as a supporting material as they give high mechanical strength and swelling resistance. Additionally, different particle and pore size availability and low costmakes these materials one of the most suitable stationary phase. In this work, chemically bonded C8 phase was synthesized by sol-gelroute and instead of toxic silicone alkoxides, non-toxic water glass was chosen as a precursor. Linking process of C8 groups to silica gel was carried out by trimethoxy(octyl)silane. The end-capping and C binding procedure was analyzed by Fourier transform infrared (FTIR) spectroscopy and morphology of C8 particles were characterized by scanning electron microscope (SEM).
Anahtar Kelime: Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık
- Aksu, A., Taskin, O.S. (2012). Organochlorine residue and toxic metal (Pb, Cd and Cr) levels in the surface sediments of the Marmara Sea and the coast of Istanbul, Turkey. Marine Pollution Bulletin, 64, 1060-1062.
- Balcioglu, E.B., Aksu, A., Balkis, N., Ozturk, B. (2014). T-PAH contamination in Mediterranean mussels (Mytilus galloprovincialis, Lamarck, 1819) at various stations of the Turkish Straits System. Marine Pollution Bulletin, 88(1), 344-346.
- Berek, D., Novák, I. (1990). Silica gel and carbon column packings for use in high-performance liquid chromatography. Chromatographia, 30(9), 582-590.
- Brown, L., Earle, M.J., Gîlea, M.A., Plechkova, N.V., Seddon, K.R. (2017). Ionic liquid–liquid chromatography: a new general purpose separation methodology. Top. Curr. Chem., 375(5), 74-81.
- Buszewski, B., Jezierska, M., Wełniak, M., Berek, D. (1998). Survey and trends in the preparation of chemically bonded silica phases for liquid chromatographic analysis. J. High Resolut. Chromatogr, 21(5), 267-281.
- Cacace, J.E., Mazza, G. (2006). Pressurized low polarity water extraction of lignans from whole flaxseed. J. Food Eng., 77(4), 1087-1095.
- Morbidelli, M., Guiochon, G., Felinger, A., Shirazi, D.G. (2006). Introduction to Fundamentals of Preparative and Nonlinear Chromatography, Ch. 1. Amsterdam: Elsevier.
- Sýkora, D., Tesařová, E., Popl, M. (1997). Interactions of basic compounds in reversed-phase highperformance liquid chromatography influence of sorbent character, mobile phase composition, and pH on retention of basic compounds. J. Chromatogr. A, 758(1), 37-51.
- Taskin, O.S., Aksu, A., Cetintasoglu, M.E., Korkmaz, N.E., Torlak, C., Balkis, N., (2017) Preparation of analytical columns and HPLC silica-based C18 packing material synthesis from non-toxic silica source. J. Liq. Chromatogr. Relat. Technol., 41(10), 583-587.
- Taskin, O.S., Kiskan, B., Aksu, A., Balkis, N., Weber, J., Yagci, Y. (2014). Polybenzoxazine: A powerful tool for removal of mercury salts from water. Chem. – Eur. J., 20(35), 10953-10958.
- Taskin, O.S., Kiskan, B., Aksu, A., Balkis, N., Yagci, Y. (2015). Preparation of microporous organic polymer through Schiff base chemistry and its potential application. Des. Monomers Polym., 18(6), 567-573.
- Taskin, O.S., Kiskan, B., Weber, J., Yagci, Y. (2015). One Pot, One Step strategy for the preparation of clickable melamine based microporous organic polymer network. Macromol. Mater. Eng., 300(11), 1116-1122.
- Taskin, O.S., Temel, B.A., Tasdelen, M.A., Yagci, Y. (2015). Synthesis of block copolymers by selective H-abstraction and radical coupling reactions using benzophenone/benzhydrol photoinitiating system. Eur. Polym. J., 62, 304-311.
- Ugelstad, J., Mórk, P.C., Kaggerud, K.H., Ellingsen, T., Berge, A. (1980). Swelling of oligomer-polymer particles. New methods of preparation. Adv. Colloid Interface Sci., 13(1), 101-140.
- Unger, K. (1972). Structure of Porous Adsorbents. Angew. Chem., 11(4), 267-278.
- Unger, K. (1979). Chapter 4 Particle characteristics. In: Journal of Chromatography Library. Elsevier.
- Unger, K. (1990) Packings and stationary phases in chromatographic techniques. Chromatogr. Sci. Ser., 8, 47-55.
- Unger, K., (1979). Chapter 2 Pore structure of silica. In: Journal of Chromatography Library. Elsevier.
- Unger, K., Scharf, B. (1976). Controlled porosity silica supports from hydrolytic polycondensation reaction of poly (ethoxysiloxane). J. Colloid Interface Sci., 55(2), 377-380.
- Yuca, N., Cetintasoglu, M.E., Dogdu, M.F., Akbulut, H., Tabanli, S., Colak, U., Taskin O.S. (2018). Highly efficient poly(fluorene phenylene) copolymer as a new class of binder for high capacity silicon anode in lithium ion batteries. Int. J. Energy Res., 42(3), 1148- 1157.
| APA | AKSU A, TAŞKİN O, CETİNTASOĞLU M, KORKMAZ N, TORLAK C, BALKİS N (2020). Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass. , 127 - 131. 10.30897/ijegeo.700599 |
| Chicago | AKSU Abdullah,TAŞKİN Omer S.,CETİNTASOĞLU Mehmet E.,KORKMAZ Nagihan E.,TORLAK Cihan,BALKİS Nuray CAGLAR Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass. (2020): 127 - 131. 10.30897/ijegeo.700599 |
| MLA | AKSU Abdullah,TAŞKİN Omer S.,CETİNTASOĞLU Mehmet E.,KORKMAZ Nagihan E.,TORLAK Cihan,BALKİS Nuray CAGLAR Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass. , 2020, ss.127 - 131. 10.30897/ijegeo.700599 |
| AMA | AKSU A,TAŞKİN O,CETİNTASOĞLU M,KORKMAZ N,TORLAK C,BALKİS N Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass. . 2020; 127 - 131. 10.30897/ijegeo.700599 |
| Vancouver | AKSU A,TAŞKİN O,CETİNTASOĞLU M,KORKMAZ N,TORLAK C,BALKİS N Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass. . 2020; 127 - 131. 10.30897/ijegeo.700599 |
| IEEE | AKSU A,TAŞKİN O,CETİNTASOĞLU M,KORKMAZ N,TORLAK C,BALKİS N "Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass." , ss.127 - 131, 2020. 10.30897/ijegeo.700599 |
| ISNAD | AKSU, Abdullah vd. "Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass". (2020), 127-131. https://doi.org/10.30897/ijegeo.700599 |
| APA | AKSU A, TAŞKİN O, CETİNTASOĞLU M, KORKMAZ N, TORLAK C, BALKİS N (2020). Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass. International Journal of Environment and Geoinformatics, 7(2), 127 - 131. 10.30897/ijegeo.700599 |
| Chicago | AKSU Abdullah,TAŞKİN Omer S.,CETİNTASOĞLU Mehmet E.,KORKMAZ Nagihan E.,TORLAK Cihan,BALKİS Nuray CAGLAR Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass. International Journal of Environment and Geoinformatics 7, no.2 (2020): 127 - 131. 10.30897/ijegeo.700599 |
| MLA | AKSU Abdullah,TAŞKİN Omer S.,CETİNTASOĞLU Mehmet E.,KORKMAZ Nagihan E.,TORLAK Cihan,BALKİS Nuray CAGLAR Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass. International Journal of Environment and Geoinformatics, vol.7, no.2, 2020, ss.127 - 131. 10.30897/ijegeo.700599 |
| AMA | AKSU A,TAŞKİN O,CETİNTASOĞLU M,KORKMAZ N,TORLAK C,BALKİS N Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass. International Journal of Environment and Geoinformatics. 2020; 7(2): 127 - 131. 10.30897/ijegeo.700599 |
| Vancouver | AKSU A,TAŞKİN O,CETİNTASOĞLU M,KORKMAZ N,TORLAK C,BALKİS N Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass. International Journal of Environment and Geoinformatics. 2020; 7(2): 127 - 131. 10.30897/ijegeo.700599 |
| IEEE | AKSU A,TAŞKİN O,CETİNTASOĞLU M,KORKMAZ N,TORLAK C,BALKİS N "Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass." International Journal of Environment and Geoinformatics, 7, ss.127 - 131, 2020. 10.30897/ijegeo.700599 |
| ISNAD | AKSU, Abdullah vd. "Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass". International Journal of Environment and Geoinformatics 7/2 (2020), 127-131. https://doi.org/10.30897/ijegeo.700599 |
