Nanomaterial development is one of the emerging issues of today’s world. Although there are several methods such as hydrothermal, wet impregnation for the preparation of these materials, sol-gel is the mostly preferred method. In sol-gel method, a precursor material is dissolved in an appropriate solvent. After mixing procedure during a certain time period, sol is treated with respect to material to be produced. In this study, nanoparticles were produced and coated on a glass surface with sol-gel and dip coating methods. As a base nanomaterial, TiO2 sol has been prepared with an experimented technique. Another sol has been prepared to dope Ag and Ni nanoparticles as an additive. The effect of experimental parameters such as mixing period, chemical addition order, type, molar rates and amounts on the attachment percentages of Ag and Ni nanoparticles on final product was compared. A total of 8 trials were carried out and the prepared sols were coated on the glass surface. The results of these experiments, used for the preparation of nanoparticles, were compared according to X-ray spectroscopy (EDX) analysis by evaluating the attachment percentage of Ag and Ni on glass surface. Moreover, X-ray diffraction (XRD) analyzes were performed for the first 5 trials and the obtained diffraction graphs were also taken into consideration. As a result of this research, most experiments have given the good attachment percentages. It was found that the type of the chemicals and the number of the reagents used for the preparation of the sol affect the last product seriously and may lead to formation of complex compounds. Furthermore, it was also found that doped compound percentages, chemical addition order into the sol and molar ratios of chemicals used in the sol are the most influential factors effecting the attachment of Ag and Ni nanoparticles on the glass surface.