Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates

GÜNAL, Merve; DERUN, Emek Moroydor; YILDIRIM, Meral; Kipcak, Azmi Seyhun; PİŞKİN, Mehmet B; ILA, Sibel

Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates

AZMİ SEYHUN KIPÇAK, (Boş)

Merve GÜNAL, (Boş)

Sibel ILA, (Boş)

Meral YILDIRIM, (Yıldız Teknik Üniversitesi, Kimya Metalurji Fakültesi, Kimya Mühendisliği Bölümü, İstanbul, Türkiye)

Mehmet B PİŞKİN, (Boş)

Emek Moroydor DERUN (Boş)

Celal Bayar Üniversitesi Fen Bilimleri Dergisi

2 0

Yıl: 2015 Cilt: 11 Sayı: 3 Sayfa Aralığı: 409 - 412 Metin Dili: İngilizce İndeks Tarihi: 29-07-2022

Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates

Öz:

Borates are attention getting chemical compounds because of their properties which leads them a wide usage area. Being sub-group of borates, potassium borates show non-linear optical properties and owing to this they can find applications in optical modulation, optical switching, optical logic and memory, signal processing. Potassium borates can be used in welding, insulation, metal refining and lubricating oil production applications, also. In this study, potassium borates were produced from potassium chloride (KCl), sodium hydroxide (NaOH) and boron oxide (B2O3) when different molar ratios of B2O3 were used to find out the optimum ratio for the synthesis at 80°C and 1 hour of reaction time. The molar ratios of reactants were examined as 1:1:3 (as KCl:NaOH: B2O3), 1:1:4, 1:1:5, 1:1:6 and 1:1:7. The identification of products and the effects of different molar ratios on the final product were determined by X-Ray Diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FT-IR) methods. According to experimental results, the Santite (KB5O8·4H2O) mineral with powder diffraction file number (pdf) code of 01-072-1688 was produced for all molar ratios whereas the optimum ratios in which highest XRD score was obtained was 1:1:7.

Anahtar Kelime:

Belge Türü: Makale Makale Türü: Araştırma Makalesi Erişim Türü: Erişime Açık

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APA	Kipcak A, GÜNAL M, ILA S, YILDIRIM M, PİŞKİN M, DERUN E (2015). Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates. , 409 - 412.
Chicago	Kipcak Azmi Seyhun,GÜNAL Merve,ILA Sibel,YILDIRIM Meral,PİŞKİN Mehmet B,DERUN Emek Moroydor Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates. (2015): 409 - 412.
MLA	Kipcak Azmi Seyhun,GÜNAL Merve,ILA Sibel,YILDIRIM Meral,PİŞKİN Mehmet B,DERUN Emek Moroydor Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates. , 2015, ss.409 - 412.
AMA	Kipcak A,GÜNAL M,ILA S,YILDIRIM M,PİŞKİN M,DERUN E Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates. . 2015; 409 - 412.
Vancouver	Kipcak A,GÜNAL M,ILA S,YILDIRIM M,PİŞKİN M,DERUN E Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates. . 2015; 409 - 412.
IEEE	Kipcak A,GÜNAL M,ILA S,YILDIRIM M,PİŞKİN M,DERUN E "Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates." , ss.409 - 412, 2015.
ISNAD	Kipcak, Azmi Seyhun vd. "Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates". (2015), 409-412.

APA	Kipcak A, GÜNAL M, ILA S, YILDIRIM M, PİŞKİN M, DERUN E (2015). Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates. Celal Bayar Üniversitesi Fen Bilimleri Dergisi, 11(3), 409 - 412.
Chicago	Kipcak Azmi Seyhun,GÜNAL Merve,ILA Sibel,YILDIRIM Meral,PİŞKİN Mehmet B,DERUN Emek Moroydor Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates. Celal Bayar Üniversitesi Fen Bilimleri Dergisi 11, no.3 (2015): 409 - 412.
MLA	Kipcak Azmi Seyhun,GÜNAL Merve,ILA Sibel,YILDIRIM Meral,PİŞKİN Mehmet B,DERUN Emek Moroydor Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates. Celal Bayar Üniversitesi Fen Bilimleri Dergisi, vol.11, no.3, 2015, ss.409 - 412.
AMA	Kipcak A,GÜNAL M,ILA S,YILDIRIM M,PİŞKİN M,DERUN E Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates. Celal Bayar Üniversitesi Fen Bilimleri Dergisi. 2015; 11(3): 409 - 412.
Vancouver	Kipcak A,GÜNAL M,ILA S,YILDIRIM M,PİŞKİN M,DERUN E Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates. Celal Bayar Üniversitesi Fen Bilimleri Dergisi. 2015; 11(3): 409 - 412.
IEEE	Kipcak A,GÜNAL M,ILA S,YILDIRIM M,PİŞKİN M,DERUN E "Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates." Celal Bayar Üniversitesi Fen Bilimleri Dergisi, 11, ss.409 - 412, 2015.
ISNAD	Kipcak, Azmi Seyhun vd. "Determination Optimum B2O3, KCl and NaOH Molar Ratios in the Synthesis of Potassium Borates". Celal Bayar Üniversitesi Fen Bilimleri Dergisi 11/3 (2015), 409-412.